On an African safari with his friend Grant, Clyde Beatty plans to buy some black-maned Numbian lions from Jo Carter but her animals are wiped out by a fire. Despite interference by rival dealer Gorman, who hopes to ruin Jo, Beatty saves her business by helping her to capture an adult gorilla. (2nd story) When Grant is bitten by a tsetse fly and falls ill, Beatty heads for the nearest hospital through the territory of the dangerous Matabeles tribe. They are captured and condemned to death by Grubbs, a white man living with the tribe and stealing their gold. Using the Matabele Boy King as a shield, Beatty and Grant make an escape and Grubbs is forced to accompany them, leaving his loot behind.

"HIS GREAT AFRICAN ADVENTURE!"